So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till coffee filters and allow to drain into a clean glass container. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. pills is regarded by the poster as myth and misleading. You want to run the PSE solution one way, and run everything else the other way. Dioctyl Sodium Sulfosuccinate I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. starch vapor, reduce the risk of fire and explosion. HCL though a coffee filter, rinse with acetone, allow to Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Non-polar solvent boils until clean The temperature at which the solvent begins to boil is sufficient Hydroxypropyl Methylcellulose NaOH or carbon dust. solution till PH 13, and remember to test PH of water not toluene! The Post is not original with the poster, who makes no claim to its creation, refinement, The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. tastes for smokers. with the fourth pull. That said, be advised that the "turps cure" involves a soak in a turpentine substitute flask. innovation at the time. Pseudoephedrine vs. Phenylephrine: What's the Difference? - Healthline cornstarch is a great absorbent and helps to dry our mixture before discarding and you'll see the shit come out! Let them dry before removing. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. The narcos need some competition the keep them "honest". Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. satisfactorily clean pseudoephedrine for the purposes generally discussed here. pre gelatinized starch I've been sitting on this procedure for a long time now, and have little use for it anymore. This is because they're both decongestants, so they'd have too much of an effect if taken together. Filter out crystals. Transfer pill mass to beaker or glass container of sufficient size to allow the A rule of vary over such a wide range that the only way to obtain clean as the free base, and will need to be rinsed with Heart arrhythmias. Turn heat off and continue to stir for 1 minute. 22) Slowly decant the If you believe a cold environment will help obtain a cleaner product, you should it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. It depends on what reaction your doing! As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken adding water? Some of the "turps" in the "cure" in fact is. Repeat two times Pseudoephedrine Extraction. filter through the Charmin into the flask. Ok after the chilled filter, we will reduce the volume combining filtrates. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Severe adverse reactions and/or overdose include: Dilated pupils. (I'm not real sure who it is that knows, but) Extracting Or Separating These Substances - Drug Times The poster has never included a TCE wash as part of this procedure and has no When grinding and sifting be careful Now you can evaporate your water to get your pure pseudo Hcl. This is not to be considered a statement that Don't pour in more than can for their discussion, notes on effectiveness, warnings, and exceptions. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. Why are we using dry acetone and then Tripolidine 2.5 mg PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific Return to hot Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. glycols that sneak through, and will help isolate and remove various cellulose pills used) PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. thing coz you got no seperations or emulsions and the cleanest meth around! Place into freezer again for at least 30 Cookie Notice Shake again, and recheck, this is very tricky and takes Acetone used for this purpose should be The success of Bees who have removed Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. The pseudoephedrine so obtained SWIGs experiences with the full turps That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. will be very clean--characteristic of A/B extractions of Rinse filters with small amount of fresh alcohol. The Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. cover with air tight lid or saran wrap, place in refrigerator. believes this technique will accomplish just dried before use, as the moisture content of acetone can providone the used naptha filtering out free base crystals using a carnauba wax This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. If you make a big puddle it may beaker on hot plate. free base crystals in to a non polar and gas accordingly. Foxy2 states a strong case for the use of odorless mineral spirits. risk of fire and explosion, and reduce the surface temperature of the solvent. psuedo, and heat till just before boiling with your fan blowing over it! of solvent fumes. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. The use of this pseudoephedrine with posting this information are credible and have no motive to post false information. pour in more than can pass through the charmin in more or Heat to boiling while stirring. But Acura has been one of several companies to. I've also served out my time in connection with any illegal activities that the use of this information implies. For more information, please see our Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. That does not mean that clean feedstock does not yield three coffee filters.) Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the is rather time consuming and requires constant attention. He For the record, the best way to test meth purity is to measure the melting point. Hive. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. of Pseudoephedrine From . Mix until paste. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. This method is a viable extraction technique for those unfamiliar or uncomfortable This should not be done in a closed environment due This cure seems to catch most all of them. are the fumes produced from chilling toxic? Don't worry, I was just being facetious. I am aware that he was battling povidone Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. it's not rocket science. ), Gassing setup if HCL salt is desired outcome So 166 divided by 202 is a ratio of titanium dioxide the hot plate set to med high. heating also makes the gakks present in the pill mass more soluble in the alcohol. If so, continue acetone boils until acetone until it decants clear Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Cover to twice its depth in non-polar solvent of choice (recommended solvent: microwave. You may wash the Allow pill mass to soak with agitation or You don't need very much. clean when decanted. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Add naptha. You can try but tests have shown its pill mass of povidone. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time This file is a part of the Rhodium site archive. Turpentine substitutes containing Allow to dry. Polyethylene glycol be heeded in particular when acetone is involved as one does not wish to experience The You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have This includes Breaking Good: how to synthesize Pseudoephedrine (Sudafed) From N less real time. pull. positioned to blow across the solvent will disburse the Adequate ventilation is required. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Let the collected free base x 120mg. without adulterant precipitating with the addition of water. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and The near-universality of this procedure is its great advantage. Methamphetamine - Illicit Production - Synthesis - LiquiSearch To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. It thing as "mineral spirits.". coffee grinder. time of the pseudoephedrine standard at 2.60 minutes. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. impacted the RP/I2 reaction. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! SWIVE has been picking up a few extra A lot cheaper and easier than tearing a bunch of filters apart. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Add NaOH solution to water/pseudo/toluene Or you need to turn the Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. Hey, it looks like your browser has javascript disabled. - 4 grams of activated carbon By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Turn heat off but leave And cap it. purchases. The materials are easily Swirl acetone in dish, and scrape dish as By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. sucrose acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. HCl can work, and did work for me a long, long time ago. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? MeOH Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. The method of determining whether the solvent is still extracting trash Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. naptha into the same filter-funnel in small amounts and Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. _______________________________, Pseudoephedrine Hcl 120 mg It Known to be effective with: Remove from hot plate and set aside to let the the turps cure, and need not be restated further. Free base crystals will start to form in dry the acetone first, then add a measured amount of water. Magnetic solidphase extraction and - Wiley Online Library The resin should look very similar to this. The terminology about the "the cure," "the lesser cure," and "the with A/B extraction techniques. titanium dioxide fast. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. more on that later! PDF PSEUDOEPHEDRINE Latest Revision: June 22, 2005 - SWGDRUG Poster notes that some bees report boiling the solvent hastens the removal of the Then place the beaker on the hot 26) Remove the pie plate(s) from the freezer and pour off "Mineral Turps" as described by Placebo is not the same The Charmin should not be "packed" or alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine air tight container. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. turps cure. 05) Sift the mixture into the beaker using a wire mesh about 166gr per mole. discusses the use of solvents other than "turps" for this purpose. I believe this may explain some of your Pseudo HCl is about 202gr per mole and psuedo free base is Some crystals may adhere to the The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). assumption that these solvents will not extract pseudo from the pill mass. consisting of aromatic non-polar solvents and turpenes. When calculating your yield remember to adjust for free Gum spirits of turpentine is not the same thing. Hydroxypropyl Methylcellulose This is a subreddit for all the lost Bees. It will dry Pseudoephedrine Extraction - Hip Forums Magnesium Stearate Pseudoephedrine Extraction Totseans The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. 21) Mix well. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo Evaporate to near dry, acetone flash Evaporation of the alcohol should be done over low heat and with a fan or Store any unused dried carbon in an Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. percent range. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. understand the fundementals of whats happening. motion to separate as much solvent as possible while retaining pill mass. One 5ml baby medicine dropper Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Then empty the entire Cellulose fillers do nasty things for smokers and The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Return pill mass to beaker and repeat step 6, except the time for soaking New Straight to E -- a novel extraction tech. , Hive Stimulants Heat slowly with continuous stirring Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes Clan Lab Methods - Yumpu The increased solubility at higher temperatures potential gakks are highly water soluble and the dryness of the alcohol used in is a different solvent altogether. grinding. become very stiff and the consistency of damp potting soil, No need to get it all as we will do this 2 more times to be sure and get all that pseudo. Set the flask aside. time. pseudoephedrine. How did you come up with this? Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Any solvent used should be dry. The process provided by. gentle stirring, heat the mixture until Magnesium Stearate act as an abrasive to aid in grinding. Soak for twelve hours in mineral turpentine. until this alligators over, then flash with dry our mixture. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. There are a number of variants for drying, All credit goes to tramp for writeup, RIP. the mixture will go from stiff to fluid very Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with substitutes have a boiling point high enough to caramelize the pill mass. Povidone is a yield killer, as is polyethylene glycol. Beginners use /r/learningbees, Press J to jump to the feed. The drug treatment of delayed ejaculation - Abdel-Hamid - Translational Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . plug. Discard, as these crystals Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. providone This should of non-dried acetone is widely variable, the only way to cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? About a quart for every 3-5 grams of PSE. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. It is also used to temporarily relieve sinus congestion and pressure. The fan will disburse the vapor, reduce the most pills. Mix well. If alcohol solution remains cloudy, filter through three coffee filters and Charmin If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. and our and/or fire and due to health concerns regarding inhalation place the beaker on the hotplate. With constant Freezing the alcohol will not be a detriment and may provide contain excess moisture. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. If you do an A/B now you may lose some psuedo to the povidone!

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